FACULTY OF PHARMACY
Pharm. D YDC) III-Year (Main) Examination, July 2017
Subject Pharmaceutical Analysis
Time 3 Hours Max. Marks: 70
Note: Answer all questions from Part A and answer any five questions from Part-B.
PART A (10 x 2 20 Marks)
1 Write the principle involved in gel filtration.
2 Define linearity and robustness.
3 Name different type of detectors use in GLC.
4 Distinguish between HPLC and HPTLC.
5 Define Hook's law and write its equation.
6 Write about the reference electrode used in potentiometry.
7 Explain the principle of separation involved in ion exchange chromatography
8 Write the composition of karlfischer reagent.
9 Explain different ions in mass spectroscopy.
10 Write the principle involved in AAS.
PART B x 10 50 Marks)
11 Write short note on
ICH guidelines
Regulatory control
12 Discuss the principle and instrumentation of IR spectroscopy.
13 Explain the principle and instrumentation of gel electrophoresis.
14 Discuss the principle and different amperometric titration.
15 Write about different analyzers used in Mass spectroscopy.
Define chemical shift and list the various factors affecting it.
16 Write the instrumentation and applications of HPTLC.
17 Explain the principle and development technique of column chromatography.
18 Describe the construction and working of X-Ray diffraction methods.