FACULTY OF PHARMACY
Pharm D III Year (Main Backlog) Examination, July 2018
Subject: Pharmaceutical Analysis
Time: 3 Hours Max.Marks: 70
Note: Answer all questions from Part A. Any Five questions from Part B.
PART A (10x2 20 Marks)
1 Write and explain ilkovic's equation.
2 Define accuracy and precision.
3 Name different type of ionization techniques in mass spectroscopy.
4 Distinguish isocratic and gradient elution.
5 Define chemical shift and list the factors influencing it.
6 Write about the reference standard used in ESR.
7 Explain the principle of separation involved in gel filtration.
8 List out ICH guidelines for quality
9 Define current voltage curve.
10 Write the principle involved in flame photometry.
PART B (50 Marks)
11 Write short notes on:
TQM 5
GLP 5
12 Write about different types of detector used in GLC with neat sketch. 10
13 Explain the working principle and instrumentation for gel electrophoresis. 10
14 Discuss different electrodes used in potentiometric titration. 10
15 Elaborate different X-ray diffraction methods. 10
16 Write the instrumentation and applications of UV-VIS spectroscopy. 10
17 Explain the principle and development techniques in paper chromatography. 10
18 Describe the construction and working of DME. 5
Write the principle and application of DTA. 5