Exam Details

Subject pharmaceutical analysis—iii
Paper
Exam / Course bachelor of pharmacy
Department
Organization Mizoram University
Position
Exam Date November, 2018
City, State mizoram,


Question Paper

BPH/VII/61
Professional Course Examination, November 2018
Pre-CBCS
7th Semester
BACHELOR OF PHARMACY
Paper No. 61
Pharmaceutical Analysis—III
Full Marks 40
Time 2 hours
The figures in the margin indicate full marks for the questions
Answer Question No. 1 and any seven from the rest
1. Choose the correct answer of the following 1×5=5
Assign the bands in the IR spectrum for —NH.
3100-3550 cm-1
1667-1640 cm-1
1740-1720 cm-1
2260-2100 cm-1
The correct order for the basic features of a mass spectrometer is
acceleration, deflection, detection, ionization
ionization, acceleration, deflection, detection
acceleration, ionization, deflection, detection
acceleration, deflection, ionization, detection
/500 1 Contd.
The proton NMR spectrum of propane will consist of
a triplet and a singlet
a triplet and a quartet
a doublet and a sextet
a triplet and a septet
UV-vis spectroscopy of organic compounds is usually concerned with
which of the following electronic transition(s)?
s
n
n and p
n
Which of the following is not true for X-rays?
Electromagnetic radiation occupying the region between the
ultraviolet and gamma rays.
X-ray diffraction methods are based on the scattering of X-ray
by electrodes.
X-rays are produced whenever matter is irradiated with a beam
of high-energy charged particles or photons.
X-ray diffraction is used to determine crystalline structure.
2. What is ISO? Write a note on ISO 9000.
3. Write a note on stability testing of new drug substances as per ICH-quality
documents. 5
4. Define validation. Write a note on validation of analytical procedures.
5. Write a note on the different types of electronic transition in UV-vis
spectroscopy. 5
/500 2 Contd.
6. Explain the different modes of vibration of molecules which are infrared
active. Write the applications of IR spectroscopy.
7. Write a note on solvent used in NMR. What are the information we get from
interpretation of 1HNMR spectrum and 13CNMR spectrum?
8. Explain mass spectrum. Write a note on the instrumentation of mass
spectrometer.
9. Write a note on the principle and the components of gas-liquid
chromatography (GLC). 5
10. Write short notes on any two of the following 2½×2=5
Emission spectroscopy
HPLC
HPTLC


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Subjects

  • anatomy, physiology and health education—i
  • basic electronics and computer applications
  • biopharmaceutics and pharmacokinetics
  • communication skills
  • general and dispensing pharmacy
  • human anatomy and physiology—i
  • medicinal chemistry—i
  • pathophysiology of common diseases
  • pharmaceutical analysis—i
  • pharmaceutical analysis—iii
  • pharmaceutical biochemistry
  • pharmaceutical business management
  • pharmaceutical inorganic chemistry
  • pharmaceutical technology—i
  • pharmaceutical unit operation—ii
  • pharmaceutics—i
  • pharmacognosy—ii
  • pharmacognosy—iv
  • pharmacognosy—vi
  • pharmacology—ii
  • pharmacology—iv
  • physical pharmacy—i
  • remedial biology
  • remedial mathematics