Exam Details
| Subject | modern pharmaceutical analytical technique | |
| Paper | ||
| Exam / Course | m.pharm. pharmaceutics | |
| Department | ||
| Organization | solapur university | |
| Position | ||
| Exam Date | May, 2018 | |
| City, State | maharashtra, solapur |
Question Paper
Master of Pharmacy (Semester (New-CBCS) Examination, 2018
(Pharmaceutical Quality Assurance)
Modern Pharmaceutical Analytical Techniques
Day and Date Thursday, 3-5-2018 Total Marks 75
Time 10.30 a.m. to 1.30 p.m.
I. Answer any five questions.
What do you mean by fluorescence and explain instrumentation of fluorimeter
Explain different rules involved in predicting fragmentation in electron impact Mass spectrometer.
What are the different types of TLC, how do you select the stationary and mobile phases
How hydrogen bonding influences IR absorption
Explain in detail Braggs law in X ray diffraction.
Write note on gel electrophoresis.
II. Answer any three questions (3×10=30)
An aromatic compound with molecular formula C7H8 shows 1H NMR, EI Mass and IR as depicted in the below figures, identify the compound.
Explain the rules to predict the fragmentation in Mass and also McLafforty rearrangement.
Describe the instrumentation and applications of DSC.
With neat labeled diagram explain instrumentation of NMR.
Explain in detail different electron transitions in UV-visible spectroscopy and how solvent influences the absorption of UV rays.
III. With neat diagram explain different parts of HPLC. 20
With suitable diagram elaborate the working of detectors of gas chromatography.
(Pharmaceutical Quality Assurance)
Modern Pharmaceutical Analytical Techniques
Day and Date Thursday, 3-5-2018 Total Marks 75
Time 10.30 a.m. to 1.30 p.m.
I. Answer any five questions.
What do you mean by fluorescence and explain instrumentation of fluorimeter
Explain different rules involved in predicting fragmentation in electron impact Mass spectrometer.
What are the different types of TLC, how do you select the stationary and mobile phases
How hydrogen bonding influences IR absorption
Explain in detail Braggs law in X ray diffraction.
Write note on gel electrophoresis.
II. Answer any three questions (3×10=30)
An aromatic compound with molecular formula C7H8 shows 1H NMR, EI Mass and IR as depicted in the below figures, identify the compound.
Explain the rules to predict the fragmentation in Mass and also McLafforty rearrangement.
Describe the instrumentation and applications of DSC.
With neat labeled diagram explain instrumentation of NMR.
Explain in detail different electron transitions in UV-visible spectroscopy and how solvent influences the absorption of UV rays.
III. With neat diagram explain different parts of HPLC. 20
With suitable diagram elaborate the working of detectors of gas chromatography.
Other Question Papers
Subjects
- advanced biopharmaceutics and pharmacokinetics
- advanced pharmaceutical analysis (old)
- advanced pharmaceutical chemistry – i (old)
- advanced pharmaceutical chemistry – ii
- advanced pharmaceutical chemistry – iii (old) (cgpa/cbcs)
- advanced pharmaceutics – ii
- advanced pharmaceutics – iii (old)
- advances in drug delivery (old)
- audits and regulatory compliance
- computer aided drug delivery system
- cosmeticology (elective)
- cosmetics and cosmeceutica
- cosmetics and cosmeceuticals
- drug delivery system
- drug design (elective) (old)
- elective : quality control (old)
- hazards and safety management
- modern pharmaceutical analytical technique
- modern pharmaceutical analytical techniques
- modern pharmaceutics
- molecular pharmaceutics (nano tech and targeted dds)
- pharmaceutical manufacturing technology
- pharmaceutical validation
- pharmaceutics (biopharmaceutics and pharmacokinetics(old) (elective)
- product development (elective)(old)
- product development and technology transfer
- quality assurance
- quality assurance techniques – i
- quality assurance techniques – ii (old)
- quality assurance techniques – iii
- quality control (old)
- quality control and quality assurance
- quality management system
- regulatory affairs
- sterile product formulation and technology
- sterile product formulation and technology (old) (elective)
- therapeutic drug monitoring (old) (elective)