Exam Details
| Subject | advanced pharmaceutical analysis | |
| Paper | paper 3 | |
| Exam / Course | m.pharm.pharmacology | |
| Department | ||
| Organization | Dr.M.G.R. Medical University | |
| Position | ||
| Exam Date | May, 2017 | |
| City, State | tamil nadu, chennai |
Question Paper
MAY 2017 Sub. Code: 2915
M.PHARM. DEGREE EXAMINATION
FIRST YEAR
BRANCH V PHARMACEUTICAL ANALYSIS
PAPER III ADVANCED PHARMACEUTICAL ANALYSIS
Q.P. Code 262915
Time Three hours Maximum 100 Marks
I. Elaborate on: x 20 40)
1. Write the significance of the analysis of elemental ions and explain the official
method for phosphorous and sulphur.
Explain the analytical method development with necessary parameters.
2. Explain the methods for the estimation of the following functional groups.
Amine Ketone.
II. Write notes on: (10 x 6 60)
1. Write the reactions and applications of Ninhydrin.
2. Write the test for effectiveness of antimicrobial preservatives.
3. Write the principle and procedure involved in the determination of opium.
4. Write the principle and procedure involved in the biological assay of Oxytocin.
5. Write the standard calibration procedure for IR spectrophotometer.
6. Suggest the various methods involved in the determination of Thiamine.
7. Explain the analysis of drugs and excipients in solid state.
8. How will you determine the Xanthine derivatives present in pharmaceutical
preparations?
9. Give the applications of Folin-Ciocalteau reagent in pharmaceutical analysis.
10.Give the principle and procedure involved in TDM.
M.PHARM. DEGREE EXAMINATION
FIRST YEAR
BRANCH V PHARMACEUTICAL ANALYSIS
PAPER III ADVANCED PHARMACEUTICAL ANALYSIS
Q.P. Code 262915
Time Three hours Maximum 100 Marks
I. Elaborate on: x 20 40)
1. Write the significance of the analysis of elemental ions and explain the official
method for phosphorous and sulphur.
Explain the analytical method development with necessary parameters.
2. Explain the methods for the estimation of the following functional groups.
Amine Ketone.
II. Write notes on: (10 x 6 60)
1. Write the reactions and applications of Ninhydrin.
2. Write the test for effectiveness of antimicrobial preservatives.
3. Write the principle and procedure involved in the determination of opium.
4. Write the principle and procedure involved in the biological assay of Oxytocin.
5. Write the standard calibration procedure for IR spectrophotometer.
6. Suggest the various methods involved in the determination of Thiamine.
7. Explain the analysis of drugs and excipients in solid state.
8. How will you determine the Xanthine derivatives present in pharmaceutical
preparations?
9. Give the applications of Folin-Ciocalteau reagent in pharmaceutical analysis.
10.Give the principle and procedure involved in TDM.